A self-propagating high-temperature synthesis method for synthesis of zinc oxide powder

Chyi Ching Hwang; Cheng Shiung Lin; Gaw Pying Wang; Cheng Hsiung Peng; Shyan Lung Chung

doi:10.1016/j.jallcom.2007.12.088

A self-propagating high-temperature synthesis method for synthesis of zinc oxide powder

Chyi Ching Hwang
, Cheng Shiung Lin
, Gaw Pying Wang
, Cheng Hsiung Peng
, Shyan Lung Chung

Department of Chemical Engineering

Research output: Contribution to journal › Article › peer-review

15 Citations (Scopus)

Abstract

A self-propagating high-temperature synthesis (SHS) method has been developed for synthesis of ZnO powder. Powders of Zn and an appropriate amount of NH₄NO₃ were mixed and pressed into a compact place in a closed chamber with air atmosphere. The combustion reaction was ignited by heating the reactant compact directly using nichrome coil, and then as-synthesized products mainly composed of tetrapod whiskers could be obtained. Both the reaction phenomenon and the product yield were affected by the reactant composition and the stacking density, which might be explained by a proposed reaction mechanism.

Original language	English
Pages (from-to)	514-523
Number of pages	10
Journal	Journal of Alloys and Compounds
Volume	467
Issue number	1-2
DOIs	https://doi.org/10.1016/j.jallcom.2007.12.088
Publication status	Published - 2009 Jan 7

All Science Journal Classification (ASJC) codes

Mechanics of Materials
Mechanical Engineering
Metals and Alloys
Materials Chemistry

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10.1016/j.jallcom.2007.12.088

Cite this

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title = "A self-propagating high-temperature synthesis method for synthesis of zinc oxide powder",

abstract = "A self-propagating high-temperature synthesis (SHS) method has been developed for synthesis of ZnO powder. Powders of Zn and an appropriate amount of NH4NO3 were mixed and pressed into a compact place in a closed chamber with air atmosphere. The combustion reaction was ignited by heating the reactant compact directly using nichrome coil, and then as-synthesized products mainly composed of tetrapod whiskers could be obtained. Both the reaction phenomenon and the product yield were affected by the reactant composition and the stacking density, which might be explained by a proposed reaction mechanism.",

author = "Hwang, \{Chyi Ching\} and Lin, \{Cheng Shiung\} and Wang, \{Gaw Pying\} and Peng, \{Cheng Hsiung\} and Chung, \{Shyan Lung\}",

note = "Funding Information: The financial support from the National Science Council of the Republic of China (Taiwan) under the grant numbers NSC 95-2221-E-014-033 and NSC 96-2623-7-606-012 is gratefully acknowledged. ",

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doi = "10.1016/j.jallcom.2007.12.088",

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T1 - A self-propagating high-temperature synthesis method for synthesis of zinc oxide powder

AU - Hwang, Chyi Ching

AU - Lin, Cheng Shiung

AU - Wang, Gaw Pying

AU - Peng, Cheng Hsiung

AU - Chung, Shyan Lung

N1 - Funding Information: The financial support from the National Science Council of the Republic of China (Taiwan) under the grant numbers NSC 95-2221-E-014-033 and NSC 96-2623-7-606-012 is gratefully acknowledged.

PY - 2009/1/7

Y1 - 2009/1/7

N2 - A self-propagating high-temperature synthesis (SHS) method has been developed for synthesis of ZnO powder. Powders of Zn and an appropriate amount of NH4NO3 were mixed and pressed into a compact place in a closed chamber with air atmosphere. The combustion reaction was ignited by heating the reactant compact directly using nichrome coil, and then as-synthesized products mainly composed of tetrapod whiskers could be obtained. Both the reaction phenomenon and the product yield were affected by the reactant composition and the stacking density, which might be explained by a proposed reaction mechanism.

AB - A self-propagating high-temperature synthesis (SHS) method has been developed for synthesis of ZnO powder. Powders of Zn and an appropriate amount of NH4NO3 were mixed and pressed into a compact place in a closed chamber with air atmosphere. The combustion reaction was ignited by heating the reactant compact directly using nichrome coil, and then as-synthesized products mainly composed of tetrapod whiskers could be obtained. Both the reaction phenomenon and the product yield were affected by the reactant composition and the stacking density, which might be explained by a proposed reaction mechanism.

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DO - 10.1016/j.jallcom.2007.12.088

M3 - Article

AN - SCOPUS:57049169752

SN - 0925-8388

VL - 467

SP - 514

EP - 523

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

IS - 1-2

ER -

A self-propagating high-temperature synthesis method for synthesis of zinc oxide powder

Abstract

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