Direct synthesis of highly stable mesoporous molecular sieves containing zeolite building units

Ayyamperumal Sakthivel; Shing Jong Huang; Wen Hua Chen; Zon Huang Lan; Kuei Hsien Chen; Hong Ping Lin; Chung Yuan Mou; Shang Bin Liu

doi:10.1002/adfm.200400038

Direct synthesis of highly stable mesoporous molecular sieves containing zeolite building units

Ayyamperumal Sakthivel
, Shing Jong Huang
, Wen Hua Chen
, Zon Huang Lan
, Kuei Hsien Chen
, Hong Ping Lin
, Chung Yuan Mou
, Shang Bin Liu

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

56 Citations (Scopus)

Abstract

A novel, one-step synthesis of a highly stable mesoporous molecular sieve (MMS-H), which has a structure analogous to MCM-48 but which contains zeolite building units, is reported. A variety of experimental techniques-X-ray diffraction (XRD), N₂ adsorption/desorption, transmission electron microscopy (TEM), Fourier-transform infrared (FTIR) spectroscopy, hyperpolarized ¹²⁹XeNMR, and solid-state ²⁷Al and ³¹P magic-angle spinning (MAS) NMR spectroscopies - have been used to characterize the framework structure, porosity, and acidity of this novel mesoporous/microporous composite material, which is also found to possess superior thermal, hydrothermal, steam, and mechanical stabilities.

Original language	English
Pages (from-to)	253-258
Number of pages	6
Journal	Advanced Functional Materials
Volume	15
Issue number	2
DOIs	https://doi.org/10.1002/adfm.200400038
Publication status	Published - 2005 Feb

All Science Journal Classification (ASJC) codes

General Chemistry
General Materials Science
Condensed Matter Physics

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10.1002/adfm.200400038

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title = "Direct synthesis of highly stable mesoporous molecular sieves containing zeolite building units",

abstract = "A novel, one-step synthesis of a highly stable mesoporous molecular sieve (MMS-H), which has a structure analogous to MCM-48 but which contains zeolite building units, is reported. A variety of experimental techniques-X-ray diffraction (XRD), N2 adsorption/desorption, transmission electron microscopy (TEM), Fourier-transform infrared (FTIR) spectroscopy, hyperpolarized 129XeNMR, and solid-state 27Al and 31P magic-angle spinning (MAS) NMR spectroscopies - have been used to characterize the framework structure, porosity, and acidity of this novel mesoporous/microporous composite material, which is also found to possess superior thermal, hydrothermal, steam, and mechanical stabilities.",

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AU - Sakthivel, Ayyamperumal

AU - Huang, Shing Jong

AU - Chen, Wen Hua

AU - Lan, Zon Huang

AU - Chen, Kuei Hsien

AU - Lin, Hong Ping

AU - Mou, Chung Yuan

AU - Liu, Shang Bin

PY - 2005/2

Y1 - 2005/2

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AB - A novel, one-step synthesis of a highly stable mesoporous molecular sieve (MMS-H), which has a structure analogous to MCM-48 but which contains zeolite building units, is reported. A variety of experimental techniques-X-ray diffraction (XRD), N2 adsorption/desorption, transmission electron microscopy (TEM), Fourier-transform infrared (FTIR) spectroscopy, hyperpolarized 129XeNMR, and solid-state 27Al and 31P magic-angle spinning (MAS) NMR spectroscopies - have been used to characterize the framework structure, porosity, and acidity of this novel mesoporous/microporous composite material, which is also found to possess superior thermal, hydrothermal, steam, and mechanical stabilities.

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Direct synthesis of highly stable mesoporous molecular sieves containing zeolite building units

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