Effects of aging on the phase transformation and sintering properties of coprecipitated Al2O3-ZrO2 powders

Chih Chen Chen, Hsing-I Hsiang, Fu Su Yen

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

In this study, the effects of aging on the crystalline phases, crystallite sizes and sintering properties of coprecipitated Al2O 3-ZrO2 powders are investigated using thermogravimetry (TG), differential thermal analysis (DTA), X-ray diffractometry (XRD), dilatometry, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Coprecipitated Al2O3-ZrO2 powder aging in the solution promoted the dissolution and reprecipitation process, which resulted in the boehmite structure subsequently transforming into bayerite. The densification and microstructural development of the coprecipitated Al 2O3-ZrO2 powders were dependent upon the aging time which shifted the θ→alpha;Al2O3 phase transformation to a higher temperature, lowered the crystallite growth rate, and prevented the occurrence of intragranular ZrO2 particles during sintering.

Original languageEnglish
Pages (from-to)13-18
Number of pages6
JournalJournal of Ceramic Processing Research
Volume9
Issue number1
Publication statusPublished - 2008 Apr 3

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Powders
Sintering
Aging of materials
Phase transitions
Crystallite size
Densification
Differential thermal analysis
X ray diffraction analysis
Thermogravimetric analysis
Dissolution
Crystalline materials
Transmission electron microscopy
Scanning electron microscopy
Temperature
aluminum oxide hydroxide

All Science Journal Classification (ASJC) codes

  • Ceramics and Composites

Cite this

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Effects of aging on the phase transformation and sintering properties of coprecipitated Al2O3-ZrO2 powders. / Chen, Chih Chen; Hsiang, Hsing-I; Yen, Fu Su.

In: Journal of Ceramic Processing Research, Vol. 9, No. 1, 03.04.2008, p. 13-18.

Research output: Contribution to journalArticle

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