TY - JOUR
T1 - Hydrothermal synthesis of monetite and hydroxyapatite from monocalcium phosphate monohydrate
AU - Jinawath, Supatra
AU - Pongkao, Dujreutai
AU - Suchanek, Wojciech
AU - Yoshimura, Masahiro
N1 - Funding Information:
The authors acknowledge the experimental assistance of Miss Suphasinee Limpanuphap, technical assistance of Doctor Seung-Wan Song and Mr. Takahiro Fujino for SEM and FT–IR respectively. The financial support from Thailand Japan Technology Transfer Project — Overseas Economic Cooperation Fund (TJTTP — OECF) and MTEC is gratefully acknowledged.
PY - 2001
Y1 - 2001
N2 - Monetite and hydroxyapatite have been synthesized by hydrothermal treatment of monocalcium phosphate monohydrate (MCPM) suspension at 160°C and 200°C. The monetite formed whiskers typically having length, diameter and aspect ratio in the range of 26-40 μm, 1-2 μm and 20-26, respectively and the hydroxyapatite shaped needle like crystals typically being in the range of 0.2-0.5 μm in length and 0.02-0.04 μm in diameter. The morphology of the crystals seems to be controlled mainly by the solubility of the reactant species. The phase of the hydrothermal product is determined by the combination of the pH and the Ca/P ratio of the aqueous solution. The whiskers obtained can be used as a bioactive reinforcement for composites.
AB - Monetite and hydroxyapatite have been synthesized by hydrothermal treatment of monocalcium phosphate monohydrate (MCPM) suspension at 160°C and 200°C. The monetite formed whiskers typically having length, diameter and aspect ratio in the range of 26-40 μm, 1-2 μm and 20-26, respectively and the hydroxyapatite shaped needle like crystals typically being in the range of 0.2-0.5 μm in length and 0.02-0.04 μm in diameter. The morphology of the crystals seems to be controlled mainly by the solubility of the reactant species. The phase of the hydrothermal product is determined by the combination of the pH and the Ca/P ratio of the aqueous solution. The whiskers obtained can be used as a bioactive reinforcement for composites.
UR - https://www.scopus.com/pages/publications/0035216615
UR - https://www.scopus.com/pages/publications/0035216615#tab=citedBy
U2 - 10.1016/S1466-6049(01)00199-4
DO - 10.1016/S1466-6049(01)00199-4
M3 - Article
AN - SCOPUS:0035216615
SN - 1466-6049
VL - 3
SP - 997
EP - 1001
JO - International Journal of Inorganic Materials
JF - International Journal of Inorganic Materials
IS - 7
ER -