Synthesis and thermal stability of SiTiCO compounds

Jow Lay Huang; Kun Chin Shih; Shou Kang Chen

doi:10.1016/0272-8842(94)90044-2

Synthesis and thermal stability of SiTiCO compounds

Jow Lay Huang, Kun Chin Shih, Shou Kang Chen

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

Abstract

Polytitanocarbosilane (PTC) was synthesized from polydimethylsilane and titanium tetrabutoxide, with α-azobis-iso-butyronitride as initiator, in a mixture of benzene and trimethylbenzene (1:1). An SiTiCO compound was produced from PTC by heat treatment in nitrogen atmosphere. The IR spectra were used to investigate the bonding structure of PTC at various temperatures. Thermal stability of the SiTiCO was also investigated.

Original language	English
Pages (from-to)	293-297
Number of pages	5
Journal	Ceramics International
Volume	20
Issue number	5
DOIs	https://doi.org/10.1016/0272-8842(94)90044-2
Publication status	Published - 1994

All Science Journal Classification (ASJC) codes

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Process Chemistry and Technology
Surfaces, Coatings and Films
Materials Chemistry

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title = "Synthesis and thermal stability of SiTiCO compounds",

abstract = "Polytitanocarbosilane (PTC) was synthesized from polydimethylsilane and titanium tetrabutoxide, with α-azobis-iso-butyronitride as initiator, in a mixture of benzene and trimethylbenzene (1:1). An SiTiCO compound was produced from PTC by heat treatment in nitrogen atmosphere. The IR spectra were used to investigate the bonding structure of PTC at various temperatures. Thermal stability of the SiTiCO was also investigated.",

author = "Huang, {Jow Lay} and Shih, {Kun Chin} and Chen, {Shou Kang}",

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AU - Shih, Kun Chin

AU - Chen, Shou Kang

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AB - Polytitanocarbosilane (PTC) was synthesized from polydimethylsilane and titanium tetrabutoxide, with α-azobis-iso-butyronitride as initiator, in a mixture of benzene and trimethylbenzene (1:1). An SiTiCO compound was produced from PTC by heat treatment in nitrogen atmosphere. The IR spectra were used to investigate the bonding structure of PTC at various temperatures. Thermal stability of the SiTiCO was also investigated.

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