Two-step oxygen injection process for growing ZNO nanorods

Yung Kuan Tseng, Hsu Cheng Hsu, Wen Feng Hsieh, Kuo Shung Liu, I. Cherng Chen

Research output: Contribution to journalArticlepeer-review

53 Citations (Scopus)

Abstract

Uniform hexagonal prismatic zinc oxide rods were grown over the entire alumina substrate at 550 °C using a two-step oxygen injection process, whether the substrates were coated with a catalyst or not. X-ray diffraction showed that all of the depositions exhibited a preferred orientation in the (002) plane. The influence of oxygen concentration was investigated by changing the oxygen flow rate. Oxygen concentration affected the size of ZnO nanorods, especially the diameter. The ZnO nanorods were further checked using high-resolution transmission electron microscopy, photoluminescence, Raman spectroscopy, and room-temperature ultraviolet lasing. The results showed that the rods were single crystals and had excellent optical properties. By observing the growth process, we found that the diameter increased slowly, but the longitudinal growth rate was very high. The growth of ZnO nanorods revealed that the uniform hexagonal prismatic ZnO nanorods were synthesized through vapor deposition growth and a self-catalyzed vapor-liquid-solid (VLS) process.

Original languageEnglish
Pages (from-to)2837-2844
Number of pages8
JournalJournal of Materials Research
Volume18
Issue number12
DOIs
Publication statusPublished - 2003 Dec

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

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