Synthesis of strontium ferrite nanoparticles by coprecipitation in the presence of polyacrylic acid

Dong Hwang Chen, Yuh Yuh Chen

研究成果: Article同行評審

71 引文 斯高帕斯(Scopus)

摘要

Strontium ferrite nanoparticles were prepared by coprecipitation in a PAA aqueous solution. The average diameter of the mixed hydroxide precipitates was 3.1 nm. From the thermal analysis by TGA/DTA and the phase analysis by XRD, it was shown that the appropriate molar ratio of Sr/Fe in aqueous solution was 1/8 and the precursor could yield pure strontium ferrite after calcination at above 700°C. The average diameters of the strontium ferrite nanoparticles calcined at 700 and 800°C were 34 and 41nm, respectively. The magnetic measurements indicated that their saturation magnetization (57-59 emu/g) reached 85-88% of the theoretical one and increased with the decrease of temperature at 5-400 K. Their coercivity values (55-67 Oe) were much lower than those reported earlier, revealing the resultant nanoparticles were superparamagnetic. All the magnetic properties observed reflected the nature of nanoparticles and also concerned with their morphology and microstructure.

原文English
頁(從 - 到)801-810
頁數10
期刊Materials Research Bulletin
37
發行號4
DOIs
出版狀態Published - 2002 3月 25

All Science Journal Classification (ASJC) codes

  • 一般材料科學
  • 凝聚態物理學
  • 材料力學
  • 機械工業

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